Circumvention of pH dependent release from ethylcellulose-coated pellets

Dressman, JB; Derbin, GM; Ismailos, G; Jarvis, C; Wheatley, TA; Et al

HERO ID

4829096

Reference Type

Journal Article

Year

1995

Language

English

HERO ID 4829096
In Press No
Year 1995
Title Circumvention of pH dependent release from ethylcellulose-coated pellets
Authors Dressman, JB; Derbin, GM; Ismailos, G; Jarvis, C; Wheatley, TA; Et al
Journal Journal of Controlled Release
Volume 36
Issue Oct 1995
Abstract IPA COPYRIGHT: ASHP To investigate the source of pH dependency of release from ethylcellulose (Aquacoat)-coated pellets, phenylpropanolamine hydrochloride pellets overcoated with ethylcellulose were examined. pH dependency of release was observed in all batches plasticized with dibutyl sebacate and column dried to an end-product temperature of 43-45DGC. However, when batches were heated for an additional 2 h in a forced air oven, or triethyl citrate was used as plasticizer, release was virtually independent of pH. Heating the product above the glass transition temperature (Tg) of the plasticized film was associated with more consistent release profiles. Contact angle measurements suggested that these effects were associated with changes in surface behavior upon heating; little change in titration data was seen. It was hypothesized that heating the product above the Tg of the plasticized film results in film relaxation, enabling even distribution of the surfactant throughout the film and thus minimizing surface effects that are associated with pH dependent release.
Is Certified Translation No
Dupe Override No
Is Public Yes
Language Text English