Aerobic Biotransformation of Fluorotelomer Thioether Amido Sulfonate (Lodyne) in AFFF-Amended Microcosms

Harding-Marjanovic, KC; Houtz, EF; Yi, S; Field, JA; Sedlak, DL; Alvarez-Cohen, L

HERO ID

3857456

Reference Type

Journal Article

Year

2015

Language

English

PMID

26042823

HERO ID 3857456
In Press No
Year 2015
Title Aerobic Biotransformation of Fluorotelomer Thioether Amido Sulfonate (Lodyne) in AFFF-Amended Microcosms
Authors Harding-Marjanovic, KC; Houtz, EF; Yi, S; Field, JA; Sedlak, DL; Alvarez-Cohen, L
Journal Environmental Science & Technology
Volume 49
Issue 13
Page Numbers 7666-7674
Abstract The aerobic biotransformation pathways of 4:2, 6:2, and 8:2 fluorotelomer thioether amido sulfonate (FtTAoS) were characterized by determining the fate of the compounds in soil and medium microcosms amended with an aqueous film-forming foam (AFFF) solution. The biotransformation of FtTAoS occurred in live microcosms over approximately 40 days and produced 4:2, 6:2, and 8:2 fluorotelomer sulfonate (FtS), 6:2 fluorotelomer unsaturated carboxylic acid (FtUCA), 5:3 fluorotelomer carboxylic acid (FtCA), and C4 to C8 perfluorinated carboxylic acids (PFCAs). Two biotransformation products corresponding to singly and doubly oxygenated forms of 6:2 FtTAoS were also identified through high resolution mass spectrometry (MS) analysis and liquid chromatography tandem-MS. An oxidative assay was used to indirectly quantify the total concentration of polyfluorinated compounds and check the mass balance. The assay produced near complete mass recovery of FtTAoS after biotransformation, with 10% (mol/mol) of the amended FtTAoS accounted for in FtS, FtCA, and PFCA products. The transformation rates of identified products appear to be slow relative to FtTAoS, indicating that some intermediates may persist in the environment. This study confirms some of the sources of FtS and PFCAs in groundwater and soil at AFFF-impacted sites and suggests that fluorinated intermediates that are not routinely measured during the biotransformation of PFASs may accumulate.
Doi 10.1021/acs.est.5b01219
Pmid 26042823
Wosid WOS:000357840300022
Url https://search.proquest.com/docview/1701495227?accountid=171501
Is Certified Translation No
Dupe Override No
Is Public Yes
Language Text English
Keyword Aqualine Abstracts; Water Resources Abstracts; ASFA 3: Aquatic Pollution & Environmental Quality; Environment Abstracts; Sulfonates; Organic acids; Liquid Chromatography; Groundwater; Mass Spectrometry; Biotransformation; Microcosms; Carboxylic acids; Chromatographic techniques; Soil Amendments; SW 5040:Data acquisition; AQ 00001:Water Resources and Supplies; Q5 08502:Methods and instruments; ENA 15:Renewable Resources-Terrestrial