New Poly(amide-imide)/Nanocomposites Reinforced Silicate Nanoparticles Based on N-pyromellitimido-L-phenyl Alanine Containing Ether Moieties

Faghihi, K; Shabanian, M; Dadfar, E

HERO ID

3577574

Reference Type

Journal Article

Year

2012

HERO ID 3577574
In Press No
Year 2012
Title New Poly(amide-imide)/Nanocomposites Reinforced Silicate Nanoparticles Based on N-pyromellitimido-L-phenyl Alanine Containing Ether Moieties
Authors Faghihi, K; Shabanian, M; Dadfar, E
Journal High Temperature Materials and Processes
Volume 31
Issue 1
Page Numbers 7-12
Abstract A series of Poly(amide-imide)/montmorillonite nanocomposites containing N-pyromellitimido-L-phenyl alanine moiety in the main chain were synthesized by a convenient solution intercalation technique. Poly(amide-imide) (PAI) 5 as a source of polymer matrix was synthesized by the direct polycondensation reaction of N-pyromellitimido-L-phenyl alanine 3 with 4,4'-diamino diphenyl ether 4 in the presence of triphenyl phosphite (TPP), CaCl2, pyridine and N-methyl-2-pyrrolidone (NMP). The resulting nanocomposite films were characterized by Fourier transform infrared spectra (FT-IR), X-ray diffraction (XRD), scanning electron microscopy (SEM) and thermogravimetric analysis (TGA). The results showed that organo-modified clay was dispersed homogeneously in PAI matrix. TGA indicated an enhancement of thermal stability of new nanocomposites compared with the pure polymer.
Doi 10.1515/HTMP.2011.122
Wosid WOS:000304747700003
Is Certified Translation No
Dupe Override No
Is Public Yes
Keyword Poly(amide-imide); nanocomposite; thermal properties; ether moieties