The pseudophase approach to assessing chemical partitioning in air-water-cyclodextrin systems

Gao, H; Blanford, WJ; Birdwell, JE

HERO ID

2551189

Reference Type

Journal Article

Year

2009

Language

English

PMID

19475975

HERO ID 2551189
In Press No
Year 2009
Title The pseudophase approach to assessing chemical partitioning in air-water-cyclodextrin systems
Authors Gao, H; Blanford, WJ; Birdwell, JE
Journal Environmental Science & Technology
Volume 43
Issue 8
Page Numbers 2943-2949
Abstract Henry's Law constants (HLCs) of several common, subsurface hydrophobic organic pollutants (HOPs) including trichloroethylene (TCE), perchloroethylene (PCE) and benzene, toluene, ethylbenzene,and o-xylene (BTEX), were measured using a static headspace phase ratio (SHPR) method over a range of temperatures (35, 45, 55, and 65 degrees C) and experimentally and operationally relevant cyclodextrin (CD) concentrations (0, 10, 20,50,and 100g L(-1)). In aqueous CD solutions, HLC values decrease according to a power law relationship with increasing CD concentration due to an apparent solubility enhancement caused by HOP partitioning to the hydrophobic cavity of CO molecules. The temperature dependence of air-water partitioning under the influence of CD was well described by the van't Hoff equation for all HOPs tested. A three-phase equilibrium model was used to interpret air-water-CD partitioning data, treating CD as a pseudophase. Our results show that HOP CD-water partition coefficients decrease linearly with increasing temperature. CD-water partition coefficients were generally independent of CID concentration, with a few exceptions. Comparison of our results for hydroxypropyl-beta-CD and TCE to those from another study showed several major discrepancies, which were attributed to differences in the experimental methods employed. Our attempt to correlate CD-water partition coefficients with HOP chemical properties indicates that correlations based on individual chemical descriptors (e.g., aqueous solubility, octanol-water partition coefficient, molecular volume or E(T) (30) polarity index) will not be sufficient to obtain accurate estimates of HOP CD-water partition coefficients for other compounds with differing chemical structures.
Doi 10.1021/es803382z
Pmid 19475975
Wosid WOS:000265172800047
Is Certified Translation No
Dupe Override No
Comments ProQuest URL: https://www.proquest.com/docview/754541542?accountid=171501&bdid=64564&_bd=r4h4%2Bh%2Bd4GHK3yaaHNNK3vRPkwE%3D
Is Public Yes
Language Text English