Ru promoted cobalt catalyst on gamma-Al2O3 support: Influence of pre-synthesized nanoparticles on Fischer-Tropsch reaction

Park, JoY; Lee, Y; Karandikar, PR; Jun, K; Bae, JW; Ha, KSu

HERO ID

1746671

Reference Type

Journal Article

Year

2011

HERO ID 1746671
In Press No
Year 2011
Title Ru promoted cobalt catalyst on gamma-Al2O3 support: Influence of pre-synthesized nanoparticles on Fischer-Tropsch reaction
Authors Park, JoY; Lee, Y; Karandikar, PR; Jun, K; Bae, JW; Ha, KSu
Journal Journal of Molecular Catalysis A: Chemical
Volume 344
Issue 1-2
Page Numbers 153-160
Abstract Effects of Ru promoted cobalt oxide nanoparticles on gamma-Al2O3 supported catalysts were studied for Fischer-Tropsch reaction. Homogeneously sized cobalt oxide nanoparticles with the different amount of ruthenium promoter were prepared by solvothermal method using oleic acid as capping agent. Pre-synthesized CoRuOx nanoparticles were then impregnated on gamma-Al2O3 support to prepare 5CoxRu/100Al(2)O(3) catalysts (5CoxRuAl), with the amount of ruthenium x = 0 to 0.1. The catalysts were characterized by XRD, TEM, TPR, EDX, H-2 chemisorption and O-2 titration methods and compared with the catalyst prepared by conventional impregnation method, i.e. i-5Co0.05RuAl. Interestingly, catalysts prepared by nanoparticle impregnation method showed higher H-2 uptake and better reducibility with the concomitant increase in the activity due to the homogeneous dispersion of the Ru promoter across entire the nanoparticles as compared to the catalyst prepared by conventional impregnation method. The intimate contact between cobalt and ruthenium enhanced the site density of cobalt which was responsible for the promotional results in the case of 5CoxRuAl catalysts. (C) 2011 Elsevier B.V. All rights reserved.
Doi 10.1016/j.molcata.2011.05.022
Wosid WOS:000292799200019
Is Certified Translation No
Dupe Override No
Comments Source: Web of Science WOS:000292799200019
Is Public Yes
Keyword CoRuOx nanoparticles; Pre-synthesis; Ru promoter; CoRu/Al2O3 catalyst; FT synthesis