Determination of thiodiglycolic acid in urine by capillary electrophoresis

Samcová, E; Kvasnicová, V; Urban, J; Jelínek, I; Coufal, P

HERO ID

1598761

Reference Type

Journal Article

Year

1999

Language

English

PMID

10431357

HERO ID 1598761
In Press No
Year 1999
Title Determination of thiodiglycolic acid in urine by capillary electrophoresis
Authors Samcová, E; Kvasnicová, V; Urban, J; Jelínek, I; Coufal, P
Journal Journal of Chromatography A
Volume 847
Issue 1-2
Page Numbers 135-139
Abstract A sensitive capillary electrophoretic method was developed for the determination of thiodiglycolic acid (TDA) in urine which avoids the pretreatment of the urine sample. Several carrier electrolytes were examined. The most suitable carrier electrolyte system consisted of potassium hydrogen phthalate (5 mM), 2-(N-morpholino)ethanesulfonic acid (50 mM) and tetradecyltrimethylammonium bromide (0.5 mM), pH 5.2. Ten times diluted fresh midstream void urine was used for the determination. In this way, the concentrations of TDA between 5 and 50 mg/l in undiluted urine samples can be determined.
Doi 10.1016/S0021-9673(98)01034-6
Pmid 10431357
Wosid WOS:000081342400017
Url https://linkinghub.elsevier.com/retrieve/pii/S0021967398010346
Is Certified Translation No
Dupe Override No
Is Public Yes
Language Text English
Keyword vinyl chloride; thiodiglycolic acid